Please use this identifier to cite or link to this item: https://doi.org/10.21256/zhaw-4221
Publication type: Article in scientific journal
Type of review: Peer review (publication)
Title: Extraction kinetics of coffee aroma compounds using a semi-automatic machine : on-line analysis by PTR-ToF-MS
Authors: Sánchez López, José Antonio
Wellinger, Marco
Gloess, Alexia N.
Zimmermann, Ralf
Yeretzian, Chahan
DOI: 10.21256/zhaw-4221
10.1016/j.ijms.2016.02.015
Published in: International Journal of Mass Spectrometry
Volume(Issue): 401
Page(s): 22
Pages to: 30
Issue Date: 25-Apr-2016
Publisher / Ed. Institution: Elsevier
ISSN: 1387-3806
1873-2798
Language: English
Subjects: Coffee; Extraction; On-line; PTR-MS
Subject (DDC): 663: Beverage technology
Abstract: The hot-water extraction process used to make an espresso coffee is affected by a large number of factors. A proper understanding of how these factors impact the profile of the final cup is important to the quality of an espresso coffee. This work examines the effect of water temperature and pressure on the extraction kinetics of volatile organic compounds (VOCs) in coffee. This was achieved by on-line monitoring of the volatiles directly from the coffee flow, using proton-transfer-reaction time-of-flight mass-spectrometry (PTR-ToF-MS). Using hierarchical cluster analysis (HCA), tentatively identified compounds were grouped into 5 families according to their time-intensity profiles. VOCs grouped into each family had similar physicochemical properties while polarity was found to be one of the main forces driving VOC extraction kinetics. The effect of pressure was studied by extracting espresso coffees at 7, 9 and 11 bar. A pressure of 11 bar resulted in an increased extraction of volatiles over the entire extraction time (25 s). To study the effect of temperature, espresso coffees were extracted at 82, 92 and 96 °C. An increase in temperature produced a significant increase in the extraction of VOCs, especially during the last part of the extraction. The effect of temperature on extractability was more pronounced for the less polar compounds.
URI: https://digitalcollection.zhaw.ch/handle/11475/5564
Fulltext version: Published version
License (according to publishing contract): CC BY-NC-ND 4.0: Attribution - Non commercial - No derivatives 4.0 International
Departement: Life Sciences and Facility Management
Organisational Unit: Institute of Chemistry and Biotechnology (ICBT)
Appears in collections:Publikationen Life Sciences und Facility Management

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Sánchez López, J. A., Wellinger, M., Gloess, A. N., Zimmermann, R., & Yeretzian, C. (2016). Extraction kinetics of coffee aroma compounds using a semi-automatic machine : on-line analysis by PTR-ToF-MS. International Journal of Mass Spectrometry, 401, 22–30. https://doi.org/10.21256/zhaw-4221
Sánchez López, J.A. et al. (2016) ‘Extraction kinetics of coffee aroma compounds using a semi-automatic machine : on-line analysis by PTR-ToF-MS’, International Journal of Mass Spectrometry, 401, pp. 22–30. Available at: https://doi.org/10.21256/zhaw-4221.
J. A. Sánchez López, M. Wellinger, A. N. Gloess, R. Zimmermann, and C. Yeretzian, “Extraction kinetics of coffee aroma compounds using a semi-automatic machine : on-line analysis by PTR-ToF-MS,” International Journal of Mass Spectrometry, vol. 401, pp. 22–30, Apr. 2016, doi: 10.21256/zhaw-4221.
SÁNCHEZ LÓPEZ, José Antonio, Marco WELLINGER, Alexia N. GLOESS, Ralf ZIMMERMANN und Chahan YERETZIAN, 2016. Extraction kinetics of coffee aroma compounds using a semi-automatic machine : on-line analysis by PTR-ToF-MS. International Journal of Mass Spectrometry. 25 April 2016. Bd. 401, S. 22–30. DOI 10.21256/zhaw-4221
Sánchez López, José Antonio, Marco Wellinger, Alexia N. Gloess, Ralf Zimmermann, and Chahan Yeretzian. 2016. “Extraction Kinetics of Coffee Aroma Compounds Using a Semi-Automatic Machine : On-Line Analysis by PTR-ToF-MS.” International Journal of Mass Spectrometry 401 (April): 22–30. https://doi.org/10.21256/zhaw-4221.
Sánchez López, José Antonio, et al. “Extraction Kinetics of Coffee Aroma Compounds Using a Semi-Automatic Machine : On-Line Analysis by PTR-ToF-MS.” International Journal of Mass Spectrometry, vol. 401, Apr. 2016, pp. 22–30, https://doi.org/10.21256/zhaw-4221.


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